Research Article
HPTLC Fingerprint Profile and Identification of Antidiabetic and Antioxidant Leads from Bauhinia rufescens L
Table 4
1H- and
13C-NMR assignments of compound 2 (700 MHz, DMSO) in comparison with reported data for rutin (quercetin-3-orutinoside) (100 MHz, CD3OD) [
27].
| Position | δH compound (2) | δH rutin | δC compound (2) | δC rutin |
| 2 | | — | 158.08 | 158.22 | 3 | | — | 134.70 | 134.52 | 4 | | — | 178.21 | 178.39 | 5 | | — | 162.88 | 162.48 | 6 | 6.44 | 6.10 s | 99.70 | 99.72 | 7 | | — | 166.0 | 166.58 | 8 | 6.77 | 6.28 s | 94.84 | 94.90 | 9 | | — | 159.06 | 158.91 | 10 | | — | 105.99 | 105.32 | 1′ | | — | 120.73 | 122.77 | 2′ | | 7.64 s | 119.34 | 117.37 | 3′ | | — | 144.00 | 144.32 | 4′ | | — | 150.00 | 150.23 | 5′ | 6.90 d | 6.85 d | 115.67 | 115.46 | 6′ | 7.77 d | 7.63 d | 120.51 | 122.47 | 1″ | 5.22–5.27 | 4.96 d | 103.69 | 103.63 | 2″ | 5.22–5.27 | 4.96 d | 76.00 | 74.64 | 3″ | 5.22–5.27 | 4.96 d | 70.65 | — | 4″ | 3.11–3.97 m | 3.20–3.90 m | 70.13 | — | 5″ | 3.11–3.97 m | 3.20–3.90 m | 70.01 | — | 1‴ | 4.69 | 4.50 d | 101.53 | 101.92 | 2‴ | 4.69 | 4.50 d | 71.79 | 71.32 | 3‴ | 4.69 | 4.50 d | | | 4‴ | 3.11–3.97 m | 3.20–3.90 m | | | 5‴ | 3.11–3.97 m | 3.20–3.90 m | | | 6‴ | 3.11–3.97 m | 3.20–3.90 m | | |
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δ = chemical shift in ppm, s = singlet, d = doublet, and m = multiplet.
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