Research Article
The Effect of Starch and Magnetite on the Physicochemical Properties of Polyurethane Composites for Hyperthermia Treatment
Table 5
DSC results of PU/starch/magnetite composites.
| | Sample code | Glass transition of soft segments | Melting of soft segments | Cold crystallization | Glass transition of hard segments | Melting of hard segments | | (°C) | (Jg-1) | (°C) | (Jg-1) | (°C) | (Wg-1) | (°C) | (Jg-1) | (°C) | (Jg-1) |
| 1 heating run | PU_0S_0M | -44 | 0.606 | 45 | 16.4 | -6 | 0.15 | — | — | 93 | 2.2 | PU_25S_0M | -47 | 2.263 | 43 | 10.9 | -3 | 0.19 | — | — | 97 | 2 | PU_50S_0M | -46 | 0.507 | 41 | 12.9 | -1 | 0.27 | — | — | — | — | PU_75S_0M | -46 | 0.591 | 36 | 11.7 | 0 | 0.17 | — | — | 108 | 1.7 | PU_100S_0M | -49 | 0.255 | 42 | 13 | — | — | 20 | 0.199 | — | — | PU_0S_1M | -39 | 0.366 | 46 | 20.6 | -8 | 0.27 | — | — | 96 | 3.2 | PU_25S_1M | -45 | 0.524 | 34 | 8.5 | -1 | 0.26 | — | — | 93 | 1.1 | PU_50S_1M | -47 | 0.317 | 34 | 7.9 | -1 | 0.29 | — | — | — | — | PU_75S_1M | -47 | 0.387 | 35 | 14.1 | -1 | 0.19 | — | — | — | — | PU_100S_1M | -48 | 0.238 | 43 | 14.1 | — | — | 19 | 0.351 | — | — | PU_0S_0.5M | -45 | 0.332 | 45 | 11.8 | -8 | 0.27 | — | — | — | — | PU_100S_0.5M | -48 | 0.039 | 44 | 12.3 | — | — | 27 | 0.298 | — | — | 2 heating run | PU_0S_0M | -36 | 0.409 | — | — | — | — | — | — | — | — | PU_25S_0M | -37 | 0.372 | — | — | — | — | — | — | — | — | PU_50S_0M | -44 | 0.418 | 39 | 11.8 | 8 | 0.22 | — | — | — | — | PU_75S_0M | -45 | 0.333 | 39 | 21 | -5 | 0.05 | — | — | — | — | PU_100S_0M | -35 | 0.331 | 39 | 22.3 | — | — | — | — | — | — | PU_0S_1M | -36 | 0.275 | — | — | — | — | — | — | 109 | 0.8 | PU_25S_1M | -38 | 0.029 | — | — | — | — | — | — | — | — | PU_50S_1M | -42 | 0.321 | 40 | 7.2 | 11 | 0.28 | — | — | — | — | PU_75S_1M | -44 | 0.224 | 39 | 19.2 | -3 | 0.09 | — | — | — | — | PU_100S_1M | -44 | 0.109 | 38 | 24.4 | -18 | 0.21 | — | — | — | — | PU_0S_0.5M | -37 | 0.419 | — | — | — | — | — | — | 89 | 1.1 | PU_100S_0.5M | -46 | 0.347 | 40 | 17.4 | — | — | — | — | — | — |
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