Research Article
Manufacturing of Filament for 4D Printing through Polyether-Type TPU/PLA Blend
Table 8
Shape memory testing of 3D-printed TPU/PLA blend samples under temperature stimulus.
| Samples | Recov. temp. (°C) | Angle (°) item | 135
| 90
| 45
| 0
|
| TPU/PLA 5 : 5 at 60°C (5 min) | | 65 | Shape | | | | | Time (s) | 15 | 50 | 90 | 230 | 70 | Shape | | | | | Time (s) | 10 | 40 | 70 | 210 | 75 | Shape | | | | | Time (s) | 15 | 40 | 60 | 200 |
| TPU/PLA 7 : 3 at 60°C (5 min) | | 65 | Shape | | | | | Time (s) | | 20 | 30 | 80 | 70 | Shape | | | | | Time (s) | | 15 | 30 | 60 | 75 | Shape | | | | | Time (s) | | 10 | 20 | 50 |
| TPU/PLA 9 : 1 at 60°C (5 min) | | 65 | Shape | | | | | Time (s) | | | 10 | 30 | 70 | Shape | | | | | Time (s) | | | 8 | 20 | 75 | Shape | | | | | Time (s) | | | 5 | 10 |
| TPU/PLA 5 : 5 at 70°C (5 min) | | 75 | Shape | | | | | Time (s) | 25 | 40 | 75 | 160 | 80 | Shape | | | | | Time (s) | 25 | 40 | 75 | 140 | 85 | Shape | | | | | Time (s) | 20 | 40 | 75 | 110 |
| TPU/PLA 7 : 3 at 70°C (5 min) | | 75 | Shape | | | | | Time (s) | 30 | 50 | 65 | 110 | 80 | Shape | | | | | Time (s) | 20 | 40 | 60 | 105 | 85 | Shape | | | | | Time (s) | 20 | 40 | 60 | 95 |
| TPU/PLA 9 : 1 at 70°C (5 min) | | 75 | Shape | | | | | Time (s) | | 10 | 20 | 80 | 80 | Shape | | | | | Time (s) | | 5 | 15 | 60 | 85 | Shape | | | | | Time (s) | | 5 | 10 | 55 |
| TPU/PLA 5 : 5 at 80°C (5 min) | | 85 | Shape | | | | | Time (s) | 40 | 55 | 90 | 150 | 90 | Shape | | | | | Time (s) | 20 | 40 | 70 | 135 | 95 | Shape | | | | | Time (s) | 20 | 40 | 65 | 110 |
| TPU/PLA 7 : 3 At 80°C (5 min) | | 85 | Shape | | | | | Time (s) | 20 | 35 | 60 | 105 | 90 | Shape | | | | | Time (s) | 20 | 30 | 55 | 100 | 95 | Shape | | | | | Time (s) | 20 | 30 | 50 | 90 |
| TPU/PLA 9 : 1 at 80°C (5 min) | | 85 | Shape | | | | | Time (s) | | 10 | 30 | 65 | 90 | Shape | | | | | Time (s) | | 10 | 25 | 60 | 95 | Shape | | | | | Time (s) | | 10 | 20 | 55 |
| TPU/PLA 5 : 5 at 90°C (5 min) | | 95 | Shape | | | | | Time (s) | 40 | 80 | 240 | | 100 | Shape | | | | | Time (s) | 20 | 60 | 210 | | 105 | Shape | | | | | Time (s) | 110 | 140 | | |
| TPU/PLA 7 : 3 At 90°C (5 min) | | 95 | Shape | | | | | Time (s) | 110 | 240 | 330 | | 100 | Shape | | | | | Time (s) | 80 | 150 | 225 | | 105 | Shape | | | | | Time (s) | 50 | 130 | 190 | |
| TPU/PLA 9 : 1 at 90°C (5 min) | | 95 | Shape | | | | | Time (s) | 10 | 40 | 70 | 120 | 100 | Shape | | | | | Time (s) | 10 | 40 | 80 | 145 | 105 | Shape | | | | | Time (s) | 10 | 80 | 115 | 155 |
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