Synthesis, X-Ray Structure, and Characterization of Catena-bis(benzoate)bis{N,N-bis(2-hydroxyethyl)glycinate}cadmium(II)

Table 1

Crystal data and structure refinement for complex 1.

Empirical formula	C26H34Cd2N2O12
Formula weight	791.35
Crystal size (mm)	0.20×0.23×0.50
Crystal system	Tetragonal
Space group	P41212
Flack parameter x	0.01(3)
θ range for data collection (^∘)	1.95≤𝜃≤25.04
a, Å	12.737(5)
b, Å	12.737(5)
c, Å	18.288(7)
𝛼^∘	90
𝛽^∘	90
𝛾^∘	90
V, Å^3	2967(2)
Z	4
𝜌calcd, g cm^-3	1.772
𝜇, mm^-1	1.498
F(000)	1584
Limiting indices, (^∘)	0≤ℎ≤15
	0≤𝑘≤15
	−21≤𝑙≤21
Reflections collected	5741
Unique reflections	2632 (𝑅int=0.0454)
Reflections used [𝐼>2𝜎(𝐼)]	2448
Parameters	246
GoF (on F ^2)	1.047
𝑅1^a	0.0273
𝑤𝑅2^a	0.0674
(Δ𝜌)max/(Δ𝜌)min, e Å^-3	0.742/−0.570

^a𝐼>2𝜎(𝐼).