Synthesis, Characterization, and Biological Activity of N′-[(Z)-(3-Methyl-5-oxo-1-phenyl-1,5-dihydro-4H-pyrazol-4-ylidene)(phenyl)methyl]benzohydrazide and Its Co(II), Ni(II), and Cu(II) Complexes

Table 2

Crystal data and structure refinement details for HL¹.

Identification code	HL^1
Formula	C24H20N4O2
Formula weight	396.44
Temperature (K)	109(2)
Wavelength (Å)	0.71073
Crystal system	Triclinic
Space group	P-1
a/Å	9.0895(2)
b/Å	10.9699(3)
c/Å	11.0637(3)
α/°	89.5410(10)
β/°	78.6940(10)
γ/°	66.0660(10)
Volume (Å^3)	985.59(4)
	2
Calculated density (Mg/m^3)	1.336
Absorption coefficient (mm^−1)	0.088
(000)	416
Crystal size (mm^3)	0.70 × 0.49 × 0.28 mm
Theta range for data collection	2.50 to 34.28°
Limiting indices	, ,
Reflections collected/unique	29726/7289 [(int) = 0.0274]
Completeness to theta	27.50° 100.0%
Absorption correction	Multiscan
Max. and min. transmission	0.9759 and 0.9412
Refinement method	Full-matrix least-squares on
Data/restraints/parameters	7289/0/278
Goodness of fit on	1.028
Final indices	,
indices (all data)	,
Largest diff. peak and hole	0.440 and −0.289 e A^−3