Research Article
Metal Complexes of a Novel Schiff Base Based on Penicillin: Characterization, Molecular Modeling, and Antibacterial Activity Study
Table 3
X-ray powder diffraction data of copper complex (1c).
| Peak number | 2θ | θ | | | | | | | % int. | in nm |
| 1 | 7.2685 | 3.63425 | 0.06338 | 0.004017 | 1 | 0 0 1 | 12.16238 | 0.2244 | 16.00 | 61.22 | 2 | 13.7483 | 6.87415 | 0.11968 | 0.014323 | 1 | 0 1 0 | 6.44119 | 0.6731 | 21.90 | 20.37 | 3 | 15.9738 | 7.9869 | 0.13894 | 0.019304 | 2 | 1 1 0 | 5.54843 | 0.0935 | 100.00 | 146.64 | 4 | 16.3780 | 8.189 | 0.14243 | 0.020286 | 10 | 1 0 −3 | 5.41242 | 0.1496 | 42.23 | 91.65 | 5 | 21.1607 | 10.58035 | 0.18361 | 0.033712 | 9 | 1 2 2 | 4.19868 | 0.2244 | 6.47 | 61.102 | 6 | 22.2011 | 11.10055 | 0.19253 | 0.03706 | 11 | 1 −1 −3 | 4.00421 | 0.2244 | 33. 02 | 61.102 | 7 | 23.5966 | 11.7983 | 0.20446 | 0.041803 | 1 | 1 0 0 | 3.77046 | 0.1870 | 28.72 | 73.323 | 8 | 26.0686 | 13.0343 | 0.22553 | 0.050863 | 6 | 1 1 2 | 3.41826 | 0.1309 | 44.73 | 104.747 | 9 | 27.7288 | 13.8644 | 0.23962 | 0.057417 | 4 | 0 2 0 | 3.21726 | 0.1496 | 38.35 | 91.654 | 10 | 28.4032 | 14.2016 | 0.24533 | 0.060186 | 10 | 1 3 0 | 3.14240 | 0.1496 | 42.24 | 91.654 | 11 | 32.3941 | 16.19705 | 0.27894 | 0.077807 | 20 | 2 0 | 2.76379 | 0.1122 | 70.54 | 122.205 | 12 | 33.2184 | 16.6092 | 0.28584 | 0.081704 | 40 | 2 0 | 2.69707 | 0.2057 | 91.73 | 66.657 | 13 | 34.5584 | 17.2792 | 0.29702 | 0.088220 | 13 | 2 0 −3 | 2.59550 | 0.2244 | 13.44 | 61.103 | 14 | 35.6718 | 17.8359 | 0.30629 | 0.093813 | 2 | 1 0 | 2.51700 | 0.2244 | 8.91 | 61.103 | 15 | 37.2666 | 18.6333 | 0.31951 | 0.102086 | 20 | 2 4 0 | 2.41287 | 0.3739 | 7.05 | 36.671 | 16 | 40.3520 | 20.176 | 0.34490 | 0.11895 | 80 | 0 4 8 | 2.23521 | 0.2617 | 23.89 | 52.394 | 17 | 43.0415 | 21.52075 | 0.36683 | 0.13456 | 9 | 1 −2 −2 | 2.10157 | 0.4487 | 11.08 | 30.5585 | 18 | 44.3550 | 22.1775 | 0.37747 | 0.14248 | 30 | 2 5 1 | 2.04234 | 0.2244 | 11.90 | 61.103 | 19 | 45.3976 | 22.6988 | 0.38588 | 0.14890 | 69 | 2 1 | 1.99783 | 0.2244 | 15.90 | 61.103 | 20 | 47.7559 | 23.87795 | 0.40478 | 0.16384 | 25 | 3 4 0 | 1.90454 | 0.1870 | 16.97 | 73.324 | 21 | 48.6714 | 24.3357 | 0.41211 | 0.16983 | 58 | 3 0 | 1.87083 | 0.2991 | 5.79 | 45.843 | 22 | 49.3094 | 24.6547 | 0.41714 | 0.174 | 18 | 3 3 0 | 1.84658 | 0.2736 | 7.79 | 50.116 | | Average particle size | 69.3474 |
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