Synthesis and Antibacterial Activity of Polyoxometalates with Different Structures

Table 1

Crystal data and structure refinements for compound 1.

Formula	C48H32Cu2N8O40W12
Fw	3710
Crystal system	Monoclinic
Space group	P21/c
a/Ǻ	26.1828(15)
b/Ǻ	11.84219(7)
c/Ǻ	23.3996(13)
α/˚	90.00
β/˚	113.74(2)
γ/˚	90.00
V/Ǻ^3	6641.2(7)
Z	4
Dc/g·cm^−3	3.711
F(000)	6600
μ/mm^−1	21.419
Rint	0.0932
Refine number of reflns/parameters/restraints	13661/991/54
R_factor_all/[I > 2sigma(I)]	0.0871/0.0456
wR_factor_ref/[I > 2sigma(I)]	0.0857/0.0745
Goodness of fit	0.954