International Journal of Analytical Chemistry / 2023 / Article / Tab 3 / Research Article
Rapid Determination of Three Organic Acids in Polygonum Vivipari Rhizoma via One Marker by HPLC-UV at Equal Absorption Wavelength and Effervescence-Assisted Matrix Solid-Phase Dispersion Table 3 The recoveries of the analytes.
Analytes Sample Original (mg) Added (mg) Found (mg) Recovery (%) Average recovery (%) RSD (%) Neochlorogenic acid 1 0.4542 0.2396 0.6976 101.55 100.99 2.69 2 0.4530 0.2396 0.6889 98.44 3 0.4533 0.2396 0.6859 97.03 4 0.4551 0.2396 0.7041 103.90 5 0.4530 0.2396 0.6968 101.73 6 0.4529 0.2396 0.7004 103.29 Chlorogenic acid 1 0.3956 0.2052 0.6026 100.90 99.85 2.87 2 0.3945 0.2052 0.5937 97.06 3 0.3948 0.2052 0.5919 96.06 4 0.3964 0.2052 0.6072 102.75 5 0.3946 0.2052 0.5986 99.43 6 0.3944 0.2052 0.6055 102.89 Cryptochlorogenic acid 1 0.1101 0.0631 0.1767 105.54 106.29 0.78 2 0.1098 0.0631 0.1773 106.90 3 0.1099 0.0631 0.1763 105.17 4 0.1103 0.0631 0.1781 107.30 5 0.1098 0.0631 0.1768 106.15 6 0.1098 0.0631 0.1771 106.71