Neonicotinoid Analysis in Sunflower (Helianthus annuus) Honey Samples Collected around Tekirdag in Turkey

Table 2

MS/MS detector parameters and retention times (RT).

Analytes	RT	Precursor ion (m/z)	Product ion (m/z)	DP (volts)	EP (volts)	CEP (volts)	CE (volts)	CXP (volts)
Dinotefuran	2.4	203.08	129.1	36	8	18	15	4
			114.1	36	8	18	17	4
Nitenpyram	2.8	271.12	225.20	36	5.5	16	15	4
			56.00	36	5.5	16	49	4
Thiamethoxam	3.0	292.00	211.10	31	11.5	16	15	4
			132.10	31	11.5	16	25	4
Clothianidin	3.2	250.07	132.00	41	7.5	14	19	4
			169.10	41	7.5	14	15	4
Clothianidin-d3 (IS)	3.2	253.01	132.00	41	8	14	23	4
Imidacloprid	3.3	256.10	290.10	36	9	14	19	4
			175.10	36	9	14	21	4
Acetamiprid	3.4	223.07	126.20	41	9	12	27	4
			99.20	41	9	12	47	4
Thiacloprid	3.7	253.06	126.20	46	12	14	29	4
			99.10	46	12	14	53	4

Confirmative ion. DP: declustering potential, EP: entrance potential, CEP: cell exit potential, CE: collision energy, CXP: collision cell exit potential, IS: internal standard.