Research Article

New Nanosized V(III), Fe(III), and Ni(II) Complexes Comprising Schiff Base and 2-Amino-4-Methyl Pyrimidine: Synthesis, Properties, and Biological Activity

Table 5

The crystal data of the complexes.

ParametersV(III) complexFe(III) complexNi(II) complex

Empirical formulaC29H27N5O2VCl2C29H27N5O2FeCl2C29H27N5O2NiCl2
Formula weight599.11604.01606.86
Crystal systemTriclinicTriclinicMonoclinic
a (Å)3.8224.6306.704
b (Å)7.3897.57811.843
c (Å)10.1388.85212.63
Alfa (°)71.59379.08090.00
Beta (°)52.656113.732101.2
Gamma (°)53.17046.04190.00
Volume of unit cell (Å3)181.66202.77983
Particle size (nm)295039