Research Article
Thermal Hazards of Synthesizing a Grignard Reagent under Different Dosing Rates
Figure 5
Thermal release, thermal accumulation, dosing of p-bromotoluene, and Tcf curves for synthesis of Grignard reagent. (a) Dosing rate of 2.0 g⋅min−1. (b) Dosing rate of 1.0 g⋅min−1. (c) Dosing rate of 0.5 g⋅min−1. Tcf1 is the maximum temperature in the induction period, and Tcf2 is the maximum temperature during the dosing period.
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