Thermal Hazards of Synthesizing a Grignard Reagent under Different Dosing Rates

Table 3

Thermal parameters for decomposition of Grignard reagent.

To (K)	Tf (K)	Φ	ΔTad (K)	ΔTad,s (K)	βm (K⋅min^−1)	TMRad (h)	ΔH (J⋅g^−1)
500.37	551.85	2.3	51.48	118.40	3.40	>24	928.57

T_o is the initial decomposition temperature, β_m is the maximum heating rate, and TMR_ad is the time required to reach the maximum heating rate.