Research Article
Stripping Voltammetric Determination of Analgesics in Their Pharmaceuticals Using Nano-Riboflavin-Modified Glassy Carbon Electrode
Table 2
Optimum experimental conditions in SWSV.
| Parameters | Range studied | Optimum value | ASA | AAP | DP | ASA | AAP | DP |
| pH | 1.0 to 13.0 | 1.0 to 13.0 | 1.0 to 13.0 | 1.0 | 1.0 | 1.0 | Accumulation potential (mV) | 750 to 950 | 500 to 750 | 300 to 600 | 850 | 600 | 550 | Accumulation time (Sec) | 5 to 60 | 5 to 60 | 5 to 60 | 10 | 30 | 10 | Initial scan potential (mV) | 200 to 700 | 0 to 400 | ā300 to 300 | 200 | 200 | ā300 | Square wave amplitude (mV) | 25 to 150 | 25 to 150 | 25 to 150 | 50 | 25 | 50 | Frequency (Hz) | 20 to 100 | 20 to 100 | 20 to 100 | 40 | 40 | 40 | Scan increment (mV) | 2 to 20 | 2 to 20 | 2 to 20 | 4 | 4 | 4 | Scan rate (mV/sec) | 10 to 80 | 10 to 60 | 20 to 80 | 60 | 40 | 50 | Stirring rate (rpm) | 50 to 250 | 50 to 250 | 50 to 250 | 250 | 250 | 250 | Rest period (Sec) | 2 to 10 | 2 to 10 | 2 to 10 | 5 | 5 | 5 |
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