Research Article

Stripping Voltammetric Determination of Analgesics in Their Pharmaceuticals Using Nano-Riboflavin-Modified Glassy Carbon Electrode

Table 2

Optimum experimental conditions in SWSV.

ParametersRange studiedOptimum value
ASAAAPDPASAAAPDP

pH1.0 to 13.01.0 to 13.01.0 to 13.01.01.01.0
Accumulation potential (mV)750 to 950500 to 750300 to 600850600550
Accumulation time (Sec)5 to 605 to 605 to 60103010
Initial scan potential (mV)200 to 7000 to 400āˆ’300 to 300200200āˆ’300
Square wave amplitude (mV)25 to 15025 to 15025 to 150502550
Frequency (Hz)20 to 10020 to 10020 to 100404040
Scan increment (mV)2 to 202 to 202 to 20444
Scan rate (mV/sec)10 to 8010 to 6020 to 80604050
Stirring rate (rpm)50 to 25050 to 25050 to 250250250250
Rest period (Sec)2 to 102 to 102 to 10555