Implementation and Validation of an Analytical Method for Lincomycin Determination in Feathers and Edible Tissues of Broiler Chickens by Liquid Chromatography Tandem Mass Spectrometry

Table 2

Monitored ion masses.

Analyte	Precursor ion (Q1 mass) (Da)	Fragment ion (Q3 mass) (Da)	Time (ms)	DP (V)	EP (V)	CE (V)	CXP (V)
Lincomycin 1	407.0	126.0	400.0	26.0	6.0	30.0	12.0
Lincomycin 2	407.0	359.0	400.0	26.0	6.0	27.0	4.0
Lincomycin D3 1	410.0	129.0	400.0	26.0	6.0	30.0	12.0
Lincomycin D3 2	410.0	362.0	400.0	26.0	6.0	27.0	12.0

Q1: quadrupole 1; Q3: quadrupole 3; Da: dalton; DP: declustering potential; EP: entrance potential; CE: collision energy; CXP: collision cell exit potential; V: volt. The precursor ion 410.0/362.0 of lincomycin D3 was used for quantification of the analyte in all samples.