Research Article

Bioguided Isolation and Structure Identification of Acetylcholinesterase Enzyme Inhibitors from Drynariae Rhizome

Table 2

13C-NMR data (500 MHz, CD3OD) of the eight flavonoids (ppm).

PositionNaringeninEriodictyolKaempferolLuteolinAstragalinLuteolin-7-O-β-D-glucosideNaringinNeoeriocitrin

1
279.178.·146.4164.3156.8164.580.579.3
342.641.9135.7102.9133.2103.044.042.9
4196.3196.0175.9181.7177.2181.8198.3197.2
5164.3163.4160.7157.6161.2161.1165.5163.6
695.894.998.299.299.699.596.596.4
7166.4166.6163.7164.5165.6162.9166.4165.2
895.195.793.594.093.994.795.395.4
9163.5162.4156.0161.5156.1156.9164.4163.2
10102.3101.8103.1103.7103.5105.3104.7103.5
1′129.9129.4121.7121.5120.1120.9130.6130.1
2′128.1114.3129.5113.9130.1113.3128.9113.4
3′115.0145.7115.1146.3115.2145.9116.1145.1
4′157.6145.0159.2149.9160.4150.5158.9145.6
5′115.3115.3115.1116.1115.8115.9116.1114.8
6′128.1117.9129.6119.2130.3119.2128.9118.0
1″99.9
2″73.1
3″76.4
4″70.8
5″82.0
6″60.6
Glc-1101.1102.4101.2
Glc-274.379.077.8
Glc-377.578.877.6
Glc-469.971.070.8
Glc-576.577.976.7
Glc-660.962.060.9
Rha-199.198.0
Rha-272.070.8
Rha-372.069.8
Rha-473.772.5
Rha-569.868.6
Rha-618.016.9