Journal of Analytical Methods in Chemistry / 2020 / Article / Tab 1 / Research Article
Volatile Components of Haplophyllum canaliculatum Boiss. by Different Extraction Procedures Table 1 Composition of volatile fractions of Haplophyllum canaliculatum obtained by hydrodistillation (HD), headspace solid-phase microextraction (HS-SPME) (PDMS fiber, 70°C, time exposure = 10 minutes), and solid-phase microwave extraction (800 W time exposure = 25 minutes).
Component name KI HD SFME HS-SPME % % Calculated KI % Calculated KI 2-Hexenal 855 0.45 ND — ND — Thujene 930 0.53 ND — ND — α -Pinene939 8.95 0.67 944.78 13.07 946.33 Camphene 954 2.18 ND — 2.40 962.93 Sabinene 975 4.11 ND — 5.34 984.94 β -Pinene979 18.9 4.11 990.34 21.13 992.66 Myrcene 991 ND ND — 5.32 995.36 δ -2-Carene1002 6.37 1.36 — 10.23 1023.14 α -Terpinene1017 0.38 ND — ND — Para-cymene 1025 0.77 ND — ND — Limonene 1029 8.4 2.25 1040.08 11.65 1041.73 β -Phellandrene1030 ND 1.16 1042.56 6.58 1044.62 1,8-Cineole 1031 13.94 5.56 1045.45 8.58 1046.69 Gamma-terpinene 1060 0.61 ND — ND — Sabinene hydrate 1070 0.38 ND — ND — Linalool 1097 1.64 1.43 1105.28 1.75 1105.72 Menth-2-en-1-ol<cis-para> 1122 1.58 1.38 1137.44 ND — Menth-2-en-1-ol<trans-para> 1141 0.83 0.90 1155.55 ND — Borneol 1169 ND ND — 1.44 1188.10 Terpinen-4-ol 1177 2.17 1.62 1196.03 ND — α -Terpineol1189 ND 0.99 1208.01 ND — Cis-piperitol 1196 0.46 ND — ND — Piperitone 1253 12.22 34.50 1281.13 5.88 1276.88 Bornyl acetate 1289 4.90 5.29 1305 ND — Pinocarvyl acetate 1312 0.52 ND — ND — Myrtenyl acetate 1327 1.11 1.08 1342.5 ND — Caryophyllene (trans) 1419 2.71 5.20 1455.02 6.58 1455.02 Elemol 1550 ND 6.32 1579.42 ND — Caryophyllene oxide 1583 4.14 9.94 1625.29 ND — Eudesmol (5-epi-7-epi-alpha) 1608 ND 1.51 1642.94 ND — Gamma eudesmol 1632 ND 1.42 1671.17 ND — Caryophylla-4 (14),8 (15)-dien5-alpha-ol 1641 1.63 5.26 — ND — α -Eudesmol1654 ND 7.94 1695.88 ND — Monoterpenes (%) 51.2 9.55 75.72 Sesquiterpenes (%) 2.71 5.2 6.58 Oxygenated compounds (%) 45.97 85.14 17.65 Total identified compounds (%) 99.88 99.89 99.95 Yield (%) 1.24 1.04 —
KI: Kovats index [
26 ];
ND: not detected.
