Research Article

Determination of Organochlorine Pesticides in Green Leafy Vegetable Samples via Fe3O4 Magnetic Nanoparticles Modified QuEChERS Integrated to Dispersive Liquid-Liquid Microextraction Coupled with Gas Chromatography-Mass Spectrometry

Table 1

Retention time and quantitative and qualitative ions of 8 OCPs.

Peak numberCompoundRetention time (min)Mass-to-charge ratio (m/z)
Quantitative ionQualitative ion

1α-HCH10.265181181, 183, 219
2β-HCH10.665109109, 181, 183
3γ-HCH10.830181181, 183, 219
4δ-HCH11.310181181, 183, 219
5p,p′-DDE15.585246246, 248, 318
6p,p′-DDD17.080235235, 237, 165
7o,p′-DDT17.190235235, 237, 165
8p,p′-DDT18.750235235, 237, 165