Research Article

Determination of Organochlorine Pesticides in Green Leafy Vegetable Samples via Fe3O4 Magnetic Nanoparticles Modified QuEChERS Integrated to Dispersive Liquid-Liquid Microextraction Coupled with Gas Chromatography-Mass Spectrometry

Table 2

Linear range, linear equation, LOD, LOQ, and enrichment factor of 8 OCPs.

OrganochlorineLinearity range (μg/kg)Linear equationCoefficient of association (r)LOD (μg/kg)LOQ (μg/kg)Enrichment factor

α-HCH1–100y = 2028x − 2280.60.99860.220.6627.4
β-HCH1–100y = 1628.1x − 3347.90.99690.210.6333.1
γ-HCH1–100y = 1413.5x + 6447.20.99870.230.6936.6
δ-HCH1–100y = 1270.8 x − 23020.99920.310.9329.3
p,p′-DDE1–100y = 1885.6x + 2662.50.99920.150.4525.2
p,p′-DDD1–100y = 6429.7 x − 121090.99880.240.7235.8
o,p′-DDT1–100y = 3444.5 x − 6867.50.99900.220.6622.8
p,p′-DDT1–100y = 1802.4 x − 1684.50.99880.320.9626.6