Binary Eluent Based Vortex-Assisted Matrix Solid-Phase Dispersion for the Extraction and Determination of Multicomponent from Musk by Gas Chromatography-Mass Spectrometry
Table 3
The contents of four compounds in 8 batches of Chinese patent medicine and 3 batches of musk samples (mean ± SD, n = 3).
Batches
Muscone (μg·mg−1)
Ethyl palmitate (μg·mg−1)
Ethyl oleate (μg·mg−1)
Ethylparaben (μg·mg−1)
XSXMN capsulea
0.236 ± 0.003
0.041 ± 0.001
0.047 ± 0.001
0.049 ± 0.002
XSXMN capsuleb
0.201 ± 0.005
0.033 ± 0.001
0.031 ± 0.001
0.035 ± 0.002
XSXMN capsulec
0.209 ± 0.003
0.035 ± 0.001
0.032 ± 0.001
0.036 ± 0.001
XJ pill
0.023 ± 0.001
0.074 ± 0.001
0.184 ± 0.006
0.042 ± 0.001
HHQL powder
2.259 ± 0.110
0.024 ± 0.001
0.207 ± 0.009
0.452 ± 0.011
XEQZ pill
0.142 ± 0.001
0.018 ± 0.001
0.066 ± 0.002
0.009 ± 0.001
SXBX pill
1.615 ± 0.065
0.846 ± 0.024
0.457 ± 0.013
0.424 ± 0.012
SXBX pill
1.538 ± 0.034
0.854 ± 0.018
0.472 ± 0.010
0.420 ± 0.007
WCA pill
0.295 ± 0.010
0.010 ± 0.001
0.077 ± 0.002
0.038 ± 0.001
WCA pill
0.290 ± 0.004
0.010 ± 0.001
0.070 ± 0.003
0.035 ± 0.001
Artificial cultivated musk (Tibet)
0.035 ± 0.001
0.027 ± 0.001
0.529 ± 0.022
ND
Artificial cultivated musk (Qing hai)
18.572 ± 0.434
0.092 ± 0.003
2.410 ± 0.074
0.014 ± 0.001
Artificial musk
73.397 ± 1.231
0.377 ± 0.007
0.717 ± 0.012
20.279 ± 0.328
Note: Xue-shuan-xin-mai-ning (XSXMN) capsule, Hong-hua-qi-li (HHQL) powder, Xiao-jin (XJ) pill, Xiao-er-qi-zhen (XEQZ) pill, She-xiang-bao-xin (SXBX) pill, and Wei-chang-an (WCA) pill. aXSXMN capsule was extracted by vortex assisted-MSPD. bXSXMN capsule was extracted by soaking. cXSXMN capsule was extracted ultrasonically.
