Hybrid Layered Crystal Comprising Polyoxometalate and Surfactant Synthesized from Reduced Mo-Blue Species

Table 1

Crystallographic data for C₁₆py-H₂Mo₈.

Chemical formula	C46H86Mo8N2O28
Formula weight	1882.69
Crystal system	Monoclinic
Space group	𝑃21/𝑐 (No. 14)
𝑎 (Å)	20.3302(4)
𝑏 (Å)	8.24345(15)
𝑐 (Å)	21.6976(15)
𝛽 (°)	116.534(8)
𝑉 (Å^3)	3253.3(2)
𝑍	2
𝜌calcd (g cm^−3)	1.922
𝑇 (K)	173(2)
𝜇 (Cu K𝛼) (mm^−1)	12.870
Number of reflections measured	36637
Number of independent reflections	5941
𝑅int	0.0405
Number of parameters	531
𝑅1 (𝐼>2𝜎(𝐼))	0.0327
𝑤𝑅2 (all data)	0.0777