Research Article

Selective Extraction of Organic Contaminants from Soil Using Pressurised Liquid Extraction

Table 3

Analytical performance on the proposed method, PLE packed with silica in the extraction cell.

CompoundLinear response ( 𝑟 2 ) Instrumental LOD ( 𝜇 g/mL)Instrumental LOQ ( 𝜇 g/mL)Precision RSD (%)
( 𝑛 = 7 )

Naphthalene
Acenaphthalene
Acenaphthene
Fluorene
Pyrene
Benzo[a]anthracene
Benzo[a]pyrene
Chlorpyrifos
Coprostanol
Cholesterol
Stigmasterol
Stigmastanol
β-Sitosterol
Phenol
Pentachlorophenol
0.9963
0.9990
0.9970
0.9965
0.9910
0.9944
0.9993
0.9975
0.9997
0.9992
0.9939
0.9998
0.9972
0.9981
0.9985
0.050
0.050
0.050
0.100
0.100
0.100
0.100
0.054
0.100
0.100
0.100
0.500
0.200
0.050
0.250
0.165
0.165
0.165
0.333
0.333
0.333
0.333
0.018
0.333
0.333
0.333
1.650
0.667
0.165
0.833
2.0
8.8
2.7
1.0
0.7
2.5
2.4
5.1
1.8
1.9
0.9
1.8
3.8
3.9
7.6