Synthesis and Characterization of Mercury(II) Complexes Containing 2,9-Dimethyl-1,10-phenanthroline by Sonochemical Method

Table 1

Experimental conditions for the preparation of the microcrystalline Hg(II) complexes.

Sample	Hg(CH3COO)2	KX, X = I, Br	Neocuprine	Sonicating time	Ultrasound power	Elemental analysis data found for; C14H12HgN2I2
1	40 mL (0.5 mM)	10 mL (1 mm) KI	10 mL (0.5 mM)	1 h	400 W	C 25.29, H 1.86, N 4.19
2	20 mL (0.1 M)	10 mL (1 mm) KI	10 mL (0.5 mM)	40 min	400 W	C 25.31, H 1.82, N 4.21
3	20 mL (0.1 M)	10 mL (1 mm) KI	10 mL (0.5 mM)	30 min	400 W	C 25.30, H 1.84, N 4.23
4	20 mL (0.1 M)	10 mL (1 mm) KI	10 mL (0.5 mM)	20 min	400 W	C 30.21, H 2.82, N 3.24
5	20 mL (0.1 M)	10 mL (1 mm) KI	10 mL (0.5 mM)	10 min	400 W	C 31.01, H 2.91, N 5.2
6	20 mL (0.1 M)	10 mL (1 mm) KI	10 mL (0.5 mM)	30 min	Without ultrasound	C 25.30, H 1.84, N 4.23