Research Article

Efficient and Rapid Solvent-Free Acetylation of Alcohols, Phenols, and Thiols Using Catalytic Amounts of Sodium Acetate Trihydrate

Table 2

Room-temperature NaOAc catalyzed acetylation of thiols.

EntryRSHRSAcTime (min.)Yield (%)a

1C6H5SHC6H5SAc1596
24-ClC6H4SH4-ClC6H4SAc3090
32-naphthyl-SH2-naphthyl-SAc4589
4C6H5CH2SHC6H5CH2SAc1090
52-furyl-CH2SH2-furyl-CH2SAc2592

Isolated yield.