Research Article

Efficient Synthesis and Characterization of Some Novel Nitro-Schiff Bases and Their Complexes of Nickel(II) and Copper(II)

Table 2

The results of the reaction for preparation of Schiff base complexes.

EntryLigandMetal(II)ProductTime (min)Yielda (%)M.p (°C)

1L1Ni(II)L1[Ni(II)]8089>350
2L2Ni(II)L2[Ni(II)]8583>350
3L3Ni(II)L3[Ni(II)]8590>350
4L4Ni(II)L4[Ni(II)]9087307
5L5Ni(II)L5[Ni(II)]9088312
6L6Ni(II)L6[Ni(II)]9087>350
7L7Ni(II)L7[Ni(II)]9085>350
8L8Ni(II)L8[Ni(II)]8083337
9L1Cu(II)L1[Cu(II)]7588335
10L2Cu(II)L2[Cu(II)]7088>350
11L3Cu(II)L3[Cu(II)]8590255
12L4Cu(II)L4[Cu(II)]8089320
13L5Cu(II)L5[Cu(II)]9082283
14L6Cu(II)L6[Cu(II)]9590>350
15L7Cu(II)L7[Cu(II)]9585302
16L8Cu(II)L8[Cu(II)]9088>350

aIsolated yields.