Research Article

Synthesis of Ruthenium Complex Based on 2,6-Bis(1-(phenyl)-1H-benzo[d]imidazol-2-yl)pyridine and 2-(1-Phenyl-1H-benzo[d]imidazol-2-yl)benzoate and Catalytical Oxidation Property of 1-(1H-Benzo[d]imidazol-2-yl)ethanol to 1-(1H-Benzo[d]imidazol-2-yl)ethanone with H2O2

Table 1

Crystal data and structure refinement for 2-(1-phenyl-1H-benzo[d]imidazol-2-yl)benzoic acid.

FormulaC20H14N2O2
Formula weight314.33
Crystal systemmonoclinic
Space groupP1211
8.6939(10)
9.5718(11)
10.0841(12)
109.609
790.49(16)
/mm−10.089
2
/gcm−31.321
Crystal size0.18 × 0.16 × 0.12
Theta range for
data collection/
2.14 to 26.34
Index ranges
328
GOF on 1.098
Reflections collected/unique6094/3151
Data/restraints/parameters3151/1/218
indices (all data)
Final indices
Max. and min.
transmission
0.9897 and 0.9846
Largest diff. peak
and hole (eA−3)
0.185 and