Synthesis, Crystal Structure, Hirshfeld Surface, and Physicochemical Characterization of New Salt Bis(2-ethyl-6-methylanilinium)tetrachloromercurate (II) [C₉H₁₄N]₂HgCl₄

Table 1

Summary of experimental details.

Crystal data
Chemical formula	[C9H14N]2HgCl4
Mr	614.81
Crystal system, space group	Monoclinic, P21/c
Temperature (K)	295
a, b, c (Å)	23.1696 (2), 25.7951 (6), 7.5980 (4)
β (°)	96.5790 (11)
V (Å^3)	4511.1 (3)
Z	8
Radiation type	Mo-Kα
μ (mm^−1)	7.30
Crystal size (mm^3)″	0.31 × 0.24 × 0.07
Data collection
Diffractometer	Nonius Kappa CCD
Tmin, Tmax	Tmin = 3.0°, Tmax = 28.0°
No. of measured, independent, and observed [I > 2σ(I)] reflections	29996, 10674, and 8223
Rint	0.093
(Sin θ/λ)max (Å^−1)	0.661
Refinement
R[F^2 > 2σ(F^2)], wR(F^2), S	0.051, 0.129, 1.04
No. of reflections	10674
No. of parameters	449
No. of restraints	5
Δρmin, Δρmax (e Å^−3)	−1.17, 1.59