Research Article

Remarkable Conversion of 2-Thioxo-2,3-dihydroquinazolin-4(1H)-ones into the Corresponding Quinazoline-2,4(1H,3H)-diones: Spectroscopic Analysis and X-Ray Crystallography

Table 1

Reaction of quinazolinthione with sodamide in methanol.

EntryCompd. No.XRTime (h)Yield (%)

19HPh1082
210HBn880
311CH3Ph1086
412NO2Ph1279
513NO2Bn1078
614ClPh881
715ClBn983
816Iph1085