Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique
Table 3
Recovery values of PAEs and bisphenols determined by analyzing packaging samples (A1 to B3) after migration test.
aPAEs and bisphenols
Spiking leves (mg L−1)
A1
A2
A3
B1
B2
B3
Mean
Rec. (%)
Mean
Rec. (%)
Mean
Rec. (%)
Mean
Rec. (%)
Mean
Rec. (%)
Mean
Rec. (%)
BFA
0
52.7 ± 1.2
—
50.7 ± 0.2
—
52.5 ± 1.5
—
50 ± 0.1
—
50.4 ± 0.5
—
50.1 ± 0.1
—
400
422.3 ± 0.3
92.4
405.8 ± 1.45
88.8
420.6 ± 0.06
92.0
400.4 ± 0.5
87.6
403.9 ± 0.10
88.4
400.8 ± 0.15
87.7
DEP
0
34 ± 1.2
—
32.2 ± 0.2
—
33.1 ± 0.7
—
32.2 ± 0.1
—
32.1 ± 1.3
—
32 ± 0.1
—
260
275.5 ± 0.1
92.9
261.1 ± 1.3
88.1
268.3 ± 1.3
90.5
261.1 ± 0.1
88.0
260.2 ± 0.2
87.9
259.3 ± 1.2
87.4
BADGE
0
26 ± 1.8
—
24.8 ± 0.9
—
24.8 ± 1.8
—
24.8 ± 0.9
—
24.8 ± 0.9
—
24.8 ± 1.8
—
200
210.5 ± 0.1
92.3
200.8 ± 0.2
88
200.6 ± 0.9
87.9
200.6 ± 0.1
87.9
200.6 ± 0.9
87.9
200.6 ± 0.9
87.9
DBP
0
31.3 ± 0.02
—
29.6 ± 0.01
—
30.6 ± 0.01
—
29.6 ± 0.01
—
29.6 ± 0.5
—
29.6 ± 0.02
—
240
254.2 ± 0.1
92.9
240.71 ± 0.01
87.9
248.1 ± 1.2
90.6
240.4 ± 0.1
87.8
240.52 ± 0.02
87.9
240.66 ± 0.01
87.9
BisDMA
0
7.2 ± 0.3
—
6.7 ± 0.3
—
6.93 ± 0.04
—
6.67 ± 0.02
—
6.7 ± 0.2
—
6.7 ± 0.3
—
55
61.3 ± 0.2
98.5
57.82 ± 0.04
92.9
59.5 ± 0.2
95.5
57.3 ± 0.2
92.1
57.3 ± 0.3
92.1
57.3 ± 0.3
92.1
DHP
0
34.7 ± 0.3
—
33.1 ± 0.4
—
33.7 ± 0.4
—
33.11 ± 0.04
—
33.12 ± 0.04
—
33.13 ± 0.03
—
260
273.1 ± 0.1
92.0
261.1 ± 0.5
87.7
266.3 ± 0.2
89.4
261.1 ± 0.2
87.7
261.1 ± 0.5
87.7
261.2 ± 0.5
87.7
DOP
0
28.75 ± 0.01
—
27.616 ± 0.001
—
28.28 ± 0.04
—
27.59 ± 0.02
—
27.586 ± 0.002
—
27.54 ± 0.01
—
220
230.1 ± 0.3
91.5
220.9 ± 0.5
87.9
226.3 ± 0.3
90.0
220.8 ± 0.1
87.8
220.7 ± 0.1
87.8
220.4 ± 0.2
87.7
Phthalic acid
0
85.7 ± 1.7
—
81.62 ± 1.9
—
85.8 ± 0.6
—
83.2 ± 0.2
—
82.7 ± 0.4
—
82.2 ± 1.4
—
300
336.7 ± 0.3
83.7
320.4 ± 0.1
79.6
337.1 ± 0.3
83.8
326.6 ± 0.1
81.1
324.6 ± 0.1
80.6
322.6 ± 0.3
80.2
aThe results are reported as BFA, DEP, BADGE, DBP, BisDMA, DHP, DOP, and phthalic acid concentrations in the analyzed solutions. bResults are expressed as the mean value ± s (n = 3). Standard deviation, s.