Journal of Chemistry

Research Article

Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique

Table 4

Recovery values of PAEs and bisphenols determined by analyzing packaging samples (C1 to E1) after migration test.


PAEs and bisphenols	Spiking leves (µg mL⁻¹)	C1		C2		C3		D1		D2		D3		E1
PAEs and bisphenols	Spiking leves (µg mL⁻¹)	Mean	Rec. (%)	Mean	Rec. (%)	Mean	Rec. (%)	Mean	Rec. (%)	Mean	Rec. (%)	Mean	Rec. (%)	Mean	Rec. (%)

BFA	0	50 ± 0.9	—	50.8 ± 0.2	—	50 ± 0.1	—	50 ± 0.9	—	50.8 ± 1.5	—	51.5 ± 1.5	—	52±±1.5	—
BFA	400	400.4 ± 1.2	87.6	406.5 ± 1.2	88.9	400.4 ± 1.5	87.6	400.3 ± 0.5	87.6	406.6 ± 0.3	89.0	412.7 ± 0.9	90.3	416.3 ± 1.5	91.1
DEP	0	32 ± 0.8	—	≤LOD	—	≤LOD	—	≤LOD	—	≤LOD	—	≤LOD	—	≤LOD	—
DEP	260	260.1 ± 0.2	87.7	260.1 ± 0.7	100.2	268.3 ± 0.1	103.4	260.1 ± 0.7	100.2	260.1 ± 0.1	100.2	260.1 ± 0.8	100.2	275.5 ± 0.8	106.2
BADGE	0	22.4 ± 0.2	—	≤LOD	—	≤LOD	—	≤LOD	—	≤LOD	—	≤LOD	—	≤LOD	—
BADGE	200	181.6 ± 0.9	80	200.8 ± 1.8	100.6	200.6 ± 0.9	100.5	200.5 ± 0.9	100.3	181.6 ± 1.8	90.8	210.5 ± 1.8	105.2	210.5 ± 0.9	105.3
DBP	0	29.6 ± 0.5	—	29.6 ± 0.5	—	29.6 ± 0.02	—	29.6 ± 0.1	—	29.6 ± 0.5	—	29.6 ± 0.02	—	29.6 ± 0.1	—
DBP	240	240.69 ± 0.01	87.9	240.6 ± 0.47	87.9	240.7 ± 0.02	87.9	240.76 ± 0.5	88.0	240.8 ± 0.1	88.07	240.45 ± 0.01	87.9	240.69 ± 0.01	87.9
BisDMA	0	6.7 ± 0.3	—	6.7 ± 0.3	—	6.66 ± 0.01	—	6.7 ± 0.2	—	6.7 ± 0.1	—	6.7 ± 0.3	—	6.63 ± 0.01	—
BisDMA	55	57.32 ± 0.04	92.1	57.3 ± 0.2	92.1	57.33 ± 0.02	92.1	57.28 ± 0.02	92.03	57.3 ± 0.2	92.1	57.32 ± 0.02	92.1	57.1 ± 0.2	91.7
DHP	0	33.11 ± 0.03	—	33.17 ± 0.04	—	33.13 ± 0.04	—	33.1 ± 0.3	—	33.1 ± 0.4	—	33.12 ± 0.04	—	33.1 ± 0.3	—
DHP	260	261.2 ± 0.4	87.7	261.2 ± 0.4	87.7	261.2 ± 0.4	87.7	261.1 ± 0.5	87.7	261.2 ± 0.3	87.7	261.2 ± 0.5	87.7	261.1 ± 0.4	87.7
DOP	0	27.6 ± 0.6	—	27.6 ± 0.2	—	27.6 ± 0.4	—	27.56 ± 0.02	—	27.58 ± 0.01	—	27.60 ± 0.01	—	27.6 ± 0.02	—
DOP	220	220.8 ± 0.9	87.9	220.711 ± 0.4	87.8	220.87 ± 0.01	87.9	220.5 ± 0.5	87.7	220.8 ± 0.3	87.8	220.86 ± 0.01	87.8	220.87 ± 0.01	87.9
Phthalic acid	0	81.9 ± 1.7	—	81.8 ± 0.6	—	82.3 ± 2.1	—	82.9 ± 1.	—	83.8 ± 0.9	—	83.03 ± 0.81	—	85.8 ± 1.5	—
Phthalic acid	300	321.7 ± 0.1	79.9	321.2 ± 0.2	79.8	323.0 ± 0.1	80.2	325.9 ± 0.3	81.0	329.0 ± 0.3	81.7	326.0 ± 0.1	81.0	336.9 ± 0.2	83.7

^aThe results are reported as BFA, DEP, BADGE, DBP, BisDMA, DHP, DOP, and Phthalic acid concentrations in the analyzed solutions. ^bResults are expressed as the mean value ± s (n = 3). Standard deviation, s.