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Journal of Chemistry
/
2022
/
Article
/
Tab 1
/
Research Article
Spectral, Structural, and Antibacterial Study of Copper(II) Complex with N
2
O
2
Donor Schiff Base Ligand and Its Usage in Preparation of CuO Nanoparticles
Table 1
Crystal data and refinement parameters for the complex Cu(H
2
L)
2
.
Compound
Cu(H
2
L)
2
Empirical formula
C
40
H
48
Cu N
6
O
8
Formula weight
802.37
Temp (K)
293.0 (2)
Wavelength
0.71073
Crystal system/space group
Triclinic, Pī
(Å)
10.9054 (16)
(Å)
13.6942 (15)
(Å)
16.2352 (19)
(°)
73.056 (10)
(°)
78.142 (11)
(°)
84.509 (10)
(Å
3
)
2268.2 (5)
4
(g/cm
3
)
1.353
(mm
-1
)
1.001
842
Crystal size (mm)
range for data collection ( ͦ)
3.562– 29.089
Index ranges
Reflections collected
3484
Independent reflections
3357 [
R
(int) =0.0070]
Absorption correction
Multiscan
Refinement method
Full-matrix least-squares on
Data/restraints/parameters
3357/426/496
Goodness of fit on
4.489
Largest difference peak and hole (e.Å
-3
)
1.380 and -1.253