Research Article

Phytoconstituent Isolation and Cytotoxicity Evaluation of the Egyptian Cassia occidentalis L. Possessing Selective Activity against Lung Carcinoma

Table 1

1H-NMR, 13C-NMR, DEPT, and HMBC (400 and 100 MHz, DMSO-d6) data of compound(9).

Carbon no.1H-NMR (m, in Hz)13C-NMRDEPTHMBC

1131.30C
27.17 (1H, br.s)104.40CH3, 4, 6
3148.40C
4148.20C
56.91 (1H, d, J = 7.6 Hz)109.0CH1, 3, 4
66.98 (1H, d, J = 7.6 Hz)123.0CH1, 2, 4
73.52 (1H, m)70.10CH-—
83.41 (1H, m)73.20CH
99a 4.20 (1H, m)62.50CH2
9b 4.46 (1H, m)
1′148.40C
2′,6′6.94 (2H, d, J = 8.1 Hz)126.10CH1′, 3′, 4′, 5′
4′131.30C
3′,5′6.87 (2H, d, J = 8.1 Hz)138.20CH1′, 4′, 7′, 2′, 6′
7′7.21 (1H, d, J = 14.8 Hz)142.40CH3′, 5′, 9′
8′6.67 (1H, d, J = 14.8 Hz)121.20CH3′, 5′, 9′
9′164.90C
9′-OH13.13 (1H, br.s.)
O-CH2-O6.02 (s)101.70CH23, 4