Monitoring the Levels of Biogenic Amines in Canned Fish Products Marketed in Ghana

Table 3

Performance of the ion-pair HPLC method for biogenic amine determination in canned mackerel.

Analyte	Regression equation	R^2	LOD	LOQ	Repeatability (%)		Recovery (%)
			(mg/kg)	(mg/kg)	Intraday	Interday	a	b	c
CAD	Y = 754848x − 566250	0.9996	0.50	1.66	4.8	7.6	82.9	83.6	90.8
PUT	Y = 1046890x − 908786	0.9997	0.43	1.43	8.9	7.7	93.4	91.6	97.3
HIS	Y = 393695x − 286586	0.9999	0.32	1.10	5.5	3.5	90.5	93.6	89.4
TYR	Y = 242031x + 96700	0.9995	0.54	1.82	8.2	3.5	92.3	96.0	94.6
AGM	Y = 162774x − 86120	0.9995	0.57	1.88	6.8	7.7	93.2	90.6	91.6