Research Article

Simultaneous Determination of Retinols and Tocols in Egg and Milk Products Based on RP-HPLC Linked with Fluorescent and Photodiode Array

Table 6

Certificated reference materials test results.

NameSRM 1869SRM 1849a
Measured value (mg/kg)Certified value (mg/kg)Measured value (mg/kg)Certified value (mg/kg)

Retinol9-cis retinol0.4519.27 ± 0.32 (for retinol)0.607.68 ± 0.23 (for retinol)
11-cis retinolNDND
13-cis retinol1.421.39
All-trans retinol18.666.60

Vitamin Eα-Tocopherol214.7217.2 ± 6.2 (for total α-tocopherol)204.70219 ± 16 (for total α-tocopherol)
β-Tocopherol3.794.22 ± 0.696.30
γ-Tocopherol99.8399.4 ± 5.1144.1
δ-Tocopherol33.2132.5 ± 2.982.3
α-Tocotrienol1.201.83
β-TocotrienolNDND
γ-Tocotrienol0.411.20
δ-Tocotrienol0.05ND

ND: not found; —: not referred.