Research Article
Rapid Analysis of 18 Flavonoids in Tea by Ultrahigh-Performance Liquid Chromatography Coupled with Quadrupole-Time of Flight Mass Spectrometry
Table 3
Linearity, LODs, and LOQs of the 18 flavonoids.
| Compound name | Recovery (%) | RSD (%) | 1LOQ | 2LOQ | 10LOQ | 1LOQ | 2LOQ | 10LOQ |
| Quercitrin | 86.7 | 88.1 | 88.5 | 1.35 | 2.11 | 1.24 | Myricetin | 81.4 | 90.2 | 81.4 | 1.45 | 1.02 | 1.65 | Isoliquiritigenin | 91.6 | 102 | 94.5 | 3.74 | 2.36 | 2.90 | Silymarin | 101 | 86.2 | 95.5 | 1.79 | 4.14 | 1.11 | Isovitexin | 84.7 | 80.9 | 88.4 | 5.37 | 2.48 | 3.45 | Vitexin | 77.6 | 79.5 | 73.8 | 2.40 | 2.15 | 2.40 | Afzelin | 80.2 | 88.0 | 88.0 | 2.13 | 3.49 | 0.340 | Luteoloside | 90.1 | 87.4 | 86.2 | 5.10 | 2.25 | 1.31 | Trilobatin | 89.7 | 84.2 | 91.2 | 1.69 | 4.59 | 1.00 | Schaftoside | 87.8 | 88.2 | 84.4 | 5.49 | 2.34 | 2.55 | Rutinum | 102 | 107 | 89.8 | 0.983 | 2.69 | 0.712 | Baimaside | 93.6 | 85.4 | 87.7 | 0.852 | 4.43 | 1.37 | Tiliroside | 85.3 | 83.7 | 85.7 | 3.51 | 3.60 | 8.05 | Camellianin A | 81.4 | 84.5 | 87.0 | 3.31 | 5.55 | 0.943 | Kaempferol | 84.8 | 91.0 | 91.2 | 3.08 | 3.48 | 1.62 | Luteolin | 82.2 | 86.5 | 88.1 | 1.68 | 1.03 | 0.544 | Quercetin | 86.4 | 93.3 | 90.3 | 3.18 | 1.19 | 0.135 | Plantagoside | 83.5 | 87.8 | 83.1 | 1.78 | 1.45 | 1.96 |
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1LOQ, 2LOQ, and 10LOQ represent the three different concentration levels: 1 × LOQ, 2 × LOQ, and 10 × LOQ. |