Research Article

Synthesis and Characterization of PVP-Stabilized Palladium Nanoparticles by XRD, SAXS, SP-ICP-MS, and SEM

Table 2

Operational parameters for XRD analysis.

SoftwareBruker Diffrac.XRD (Version 4.0)
Bruker Diffrac.EVA (Version 4.1)
Scan typeCoupled two theta/theta
Theta20°-42.5°
2 theta40°-85°
Step size15°
Time per step240 s
Measurement time960 s
Steps4
Collimator0.5 mm