Quantitative Analysis of Oxygen Gas Exhausted from Anode through In Situ Measurement during Electrolytic Reduction

Figure 5

Photographs after electrolysis: (a) cathode (inset: reduction products); (b) anode shroud; (c) Pt anode and its electrical conductor; (d) inner crucible containing the salt; (e) side view of the top flange; and (f) bottom view of the top flange.

(a)

(b)

(c)

(d)

(e)

(f)